Friday, 4 October 2013

Self Cleaning Textiles

ABSTRACT
       Now a day’s people are very busy in their work that they do not have time for clean their daily wear cloths also people who are working in kitchens having headek to wash their garments. Also military peoples have to survive in such drastic condition that they cannot wash their cloths. Nanotechnology provides a new concept self cleaning textiles which gives self cleaning as well as fresh cloths every day.
        Water and soil repellency has been one of the major targets for fiber and textile scientists and manufacturers for centuries. Combinations of new materials for fiber production with a variety of surface treatments have been developed to reach the condition of limited wet ability. This paper gives the concept behind the self cleaning textiles, different surface treatments based on nano technology, application of  self cleaning textiles problems and limitations of  self cleaning textiles.
INTRODUCTION:-
       Finishes that repel water, oil and dry dirt are important in all parts of the textile market – for clothing, home and technical textiles. Water repellency is achieved using different product groups, but oil repellency is attained only with fluorocarbon polymers. They are modified to have a wide range of properties to fit the different demands of the users and the intended purpose. This is one of the most interesting new developments of chemical finishing.
       The oldest repellent finish is to repel water. The purpose of this finish is self evident. Drops of water should not spread on the surface of the textile and should not wet the fabric. The drops should stay on the surface and easily drip off. Similarly, oil repellent finishes should prevent oily fluids from wetting treated textiles. In a similar manner, soil-repellent finishes should protect textiles from both dry and wet soils. In all cases, the air permeability of the finished fabric should not be significantly reduced.  
       In addition to the desired repellency effects, other undesirable fabric properties are often found with repellent finishes. These include problems with static electricity, poor soil removal in aqueous laundering, stiffer fabric hand, greying (soil redeposition) during aqueous laundering and increased flammability. Some fabric properties that are often improved by repellent finishes include better durable press properties, more rapid drying and ironing, and increased resistance to acids, bases and other chemicals.
Mechanisms of repellency
       Repellent finishes achieve their properties by reducing the free energy at fibre surfaces. If the adhesive interactions between a fibre and a drop of liquid placed on the fibre are greater than the internal cohesive interactions within the liquid, the drop will spread. If the adhesive interactions between the fibre and the liquid are less than the internal cohesive interactions within the liquid, the drop will not spread. Surfaces that exhibit low interactions with liquids are referred to as low energy surfaces. Their critical surface energy or surface tension γC must be lower than the surface tension of the liquid γL (the internal cohesive interaction) that is repelled. γL of water, at 73 mN m–1, is two to three times greater than γL of oils (20– 35 mN m–1). Therefore, oil repellency finishes with fluorocarbons (γC = 10–20 mN m–1) always achieve water repellency, but fluorine-free products, for example silicones (γC = 24–30 mN m–1) will not repel oil.7 Low energy surfaces also provide a measure of dry soil repellency by preventing soil particles from strongly adhering to fibre surfaces. This low interaction allows the soil particles to be easily dislodged and removed by mechanical action.
WHAT IS SELF CLEANING TEXTILES:
           The self-cleaning fabrics have a nano film coating of titanium dioxide nanoparticles  which can break down dirt molecules, pollutants, and microorganisms when exposed to visible and UV light. Clothes made this way could be cleaned by simply exposing them to sunlight. Scientists have developed a method for applying the thin film of titanium dioxide to cotton easily and inexpensively. With their method, self-cleaning fabrics could be produced commercially and for public use. The anothes method of manufacturing self cleaning textiles is application of silver nano particals on the besis of lotus leave surface structure.   The scientists note that self-cleaning fabrics could be especially useful for people who don't have the time or means for washing their clothes, such as military personnel or hikers





The Lotus Effect: biomimetic ultraphobic surfaces
       Biomimetics mimics naturally occurring biological mechanisms with modification, to produce useful imitative synthetic items using conventional methods available to science and technology. The Lotus Effect has been named after the unusual properties of the leaf surfaces of the lotus plant, which are remarkably water-repellent and soil-repellent. The surface of the lotus leaf is covered by a thin extracuticellular membrane termed the cuticle, which is covered by waxes forming characteristic microstructures due to self-organisation. On smooth wax layers (surface area contact 10%) the contact angle of water may reach 110°, but because of the surface roughness of the wax layer, whose dimensions can be measured in micrometres, a very pronounced super hydrophobicity is generated with contact angles up to 170° and surface area contact as low as 7%. (As an analogy, imagine a mercury droplet lying on a bed of nails or a pimple rubber mat.) As a result, the area for adhesion of water is markedly diminished and air is enclosed between the droplets and the wax crystals.
       A similar situation holds true for particles that are located on the surface of the lotus plant leaf. The contact angle between the particle and the surface is minimised, which results in the adhesion of particles to the water surface  Independent of their size and chemical nature, contaminants are removed from such optimised surfaces with only a small amount of water.

       This remarkable self-cleaning effect is currently being harnessed to transfer the Lotus Effect into products with bio mimetic self-cleaning surfaces. A façade paint suitable as an ‘anti-graffiti’ surface has already been devised and roof tiles and wood paints are currently under development. It is conceivable that within the next decade the application of the Lotus Effect using nanotechnology, precision engineered polymers and suitable application methods could be used to provide a new generation of fabrics with ultraphobic surfaces. These would undoubtedly be expensive but would possess very high levels of water- and oil-repellency and outstanding soil- and stain-repellency properties. However, the adhesion of such polymers to the fibre surface and their durability to abrasion, wear, laundering and dry-cleaning would have to be appropriate for the end-use.

Self Cleaning Using Nano Technology:-
       There are basically two types of self-cleaning surfaces involving nanotechnology. In the first place extremely water repellent, microscopically rough surfaces: dirt particles can hardly get a hold on them and are, therefore, removed by rain or by a simple rinse in water .The second example is given by photo-catalytic layers: due to a layer of nanocrystalline titanium oxide, fouling organic material is destroyed by solar irradiation.  Self-cleaning, deodorant and anti-VOC (volatile organic compounds) effects are possible when modifying the surface of textiles before anchoring them on TiO2. Physical methods like RF-plasma and vacuum-UV have been used to introduce carboxylic groups in wool-polyamide5 and cotton6. The TiO2 forms a complex with the -COOH groups retaining their oxidative action under solar irradiation in the presence of water vapor and air. This leads to self-cleaning effects and to the destruction of organic compounds like wine, coffee, make up, grease etc. Chemical spacers have also been used to attach TiO2 to fabrics, anchoring this semiconductor on one carboxyl and condensing the surface -TiOH with the second carboxyl-group.

       Dirt adheres to the fibers of most fabrics. To clean the fabrics, people typically put them in the washer or send them to the dry cleaners. But the water-repellency of fabrics made with the new coating is superior and makes it easier to keep dirt from accumulating, because water that is applied to the garment rolls off and takes the dirt with it. Suits made with the new coating could simply be sprayed clean or wiped with a damp cloth to remove the dirt, the researcher says. If desired, the fabric can still be cleaned by conventional means, including washing as well as dry cleaning, without harming the coating, he notes. In addition to suits, the new coating could be applied to hospital garments, sportswear, military uniforms and rain coats. Other possible applications include awning material for outdoor campers, fabrics for lawn furniture and convertible tops for cars.


Application of photo catalytic layer of titanium di oxide
        The fabric is coated with a thin layer of titanium dioxide particles that measure only 20 nanometers in diameter. When this semi-conductive layer is exposed to light, photons with energy equal to or greater than the band gap of the titanium dioxide excite electrons up to the conduction band. The excited electrons within the crystal structure react with oxygen atoms in the air, creating free-radical oxygen. These oxygen atoms are powerful oxidizing agents, which can break down most carbon-based compounds through oxidation-reduction reactions. In these reactions, the organic compounds (i.e. dirt, pollutants, and micro organisms) are broken down into substances such as carbon dioxide and water. Since the titanium dioxide only acts as a catalyst to the reactions, it is never used up. This allows the coating to continue breaking down stains over and over.
       TiO2 is acts as photo catalyst layer which destructs the dirt particles photo catalytically. The durability of this nano layer is very good up to 40-50 washing cycles.    The simple process sequence for applying the nano layer of Tio2 film is as
Pad                   dry                 cure
Working of self cleaning photo catalytic layer:
 
       The self-cleaning fabrics work using the photocatalytic properties of titanium dioxide, compound used in many new nanotechnology solar cell applications.   The fabric is coated with a thin layer of titanium dioxide particles that measure only 20 nanometers in diameter. When this semi-conductive layer is exposed to light, photons with energy equal to or greater than the band gap of the titanium dioxide excite electrons up to the conduction band. The excited electrons within the crystal structure react with oxygen atoms in the air, creating free-radical oxygen. These oxygen atoms are powerful oxidizing agents, which can break down most carbon-based compounds through oxidation-reduction reactions. In these reactions, the organic compounds (i.e. dirt, pollutants, and micro organisms) are broken down into substances such as carbon dioxide and water. Since the titanium dioxide only acts as a catalyst to the reactions, it is never used up. This allows the coating to continue breaking down stains over and over.
Reactions taking place during self cleaning:
          Titanium dioxide is a photocatalyst; when it is illuminated by light of energy higher than its band gap, electrons in TiO2 will jump from the valence band to the conduction band, and the electron (e–) and electric hole (h+) pairs will form on the surface of the photocatalyst. The negative electrons and oxygen will combine to form O2 –. radical ions, whereas the positive electric holes and water will generate hydroxyl radicals OH.. Since both products are unstable chemical entities.  The following reactions show the photo catalysis of the titanium di oxide treated fabric.






Application of silver nano particals for self cleaning :
                 Application of silver nano particles on textile surface is working as a phenomenon of lotus leaf which does not absorb the water as well as do not adhere the organic matter on its surface Similarly silver nano particals can be applied on the surface of textile. These particals canbe applied on the surface with plymer film (polyglycidyle methycrylate) which ensures that silver nano particals are get fixed on textile surface. These silver particals can be applied to silk, cotton, viscose etc. but the concept is same as that of lotus plant. The nano particals are applied on to the surface of textile by using simple finishing method pad-dry-cure. The following diagram shows applied nano particles on the textile surface
                              
Lotus leaf and a SEM image of its surface                       silver nano particals applied on textile material

Working of textile surface treated with silver nano particals :
      A highly water-repellant coating made of silver nanoparticles that can be used to produce suits and other clothing items that offer superior resistance to dirt as well as water and require much less cleaning than conventional fabrics. Nano-Tex improves the water-repellent property of fabrics by creating nanowhiskers, which are made of hydrocarbons and have about 1/1000 of the size of a typical cotton fiber. They are added to the fabric to create a peach fuzz effect without lowering the strength of cotton.
        Untreated surface                       Treated surface                                                               
                           
       The diagram shows that the two textile surface one which is treated with silver nano particals and other is not treated with silver nano particals.
The untreated surface having dust particals, when water droplates rolls over it do not get washed off because dust particals are adhere by textile surface. While treated textile surface do not adheres the dust particals hnce when water particals rolls over it dust get washed off. In fig. (b) Silver nano particals treated surface shows self cleaning property.

Slef-cleaning sportswear Self cleaning textile in sport wear:
       Muddy sports kit, the bane of parents with active children, may be heading for the laundry. Scientists have produced a coating that could make shirts and football shorts self cleaning means which can either washed easily or do not allow to develop the bacteria’s on fiber surface as shown in figure .   The "self-cleaning" process makes fabrics repel water, resist stains and even kill off the bacteria that grow in sweat and make clothes smell. As a result, kit could be worn repeatedly between washes, the distinctive aroma of kit bags gone for ever – even performance on the field could be enhanced.
       Scientists working for the US Air Force have already produced T-shirts and underwear that can be worn for weeks at a time without washing, and the technology has now been licensed to a London company, Alexium, to develop for civilian applications

Limitations of self cleaning fabric:

       Breakthroughs in nanotechnology have made self-cleaning fabrics both practical and economical. With commercial production making the technology readily available to the masses, will washing machines and laundry detergent become obsolete? 
       There are several factors limiting how quickly current self cleaning fabric would be able to break down organic compounds. Sunlight is the best source of light for activating the self-cleaning process. A ketchup-stained shirt would have to be left outside in the sun for at least a day in order to remove the stain. However, for military persons or hikers, who are outside in the sun for long periods of time without the time or means to clean their clothes, self-cleaning fabric would be ideal. It's also important to note that the newly developed method for producing self-cleaning fabric has only been developed for cotton.  Further research would be required to test ways of applying titanium dioxide nanofilms to other textiles.

Problems with Self-Cleaning Fabric :
            The main reasons that self-cleaning fabrics require a lot of time to break down stains is because titanium dioxide is very inefficient at using energy from sunlight. The titanium dioxide serves as a catalyst for the break down of dirt molecules by providing electrons that oxidize oxygen molecules in the surrounding air. The electrons are freed from the titanium dioxide via the photoelectric effect. But because of titanium dioxide's high band gap energy, only high energy blue and UV light photons have enough energy to excite electrons to the conduction band. High energy blue and UV light only make up 3% of the solar spectrum, so titanium dioxide can only use a very small portion of the sun's energy to break down stains.
             Excitation of electrons to the conduction band is only the beginning of the cleaning process. These electrons must then react with oxygen atoms, which then react with the dirt particles. All of these reactions are limited by access to and the amount of freed electrons in the titanium dioxide. So for a large stain, a lot of light energy is needed before the fabric can fully break it down.





CONCLUSION
       The realization of self-cleaning properties on textile surfaces by using the nanotechnology includes a vast potential for the development of new materials or new products and applications for known materials. The opening of new application fields for textiles will lead to a new growth stage. For the growing market of technical textiles a further increase in production volume, sales and application fields can be expected by successful transfer of the self cleaning effect on textile materials. Structure based soil and water-repellent properties lead to an efficient use of materials and are therefore in agreement with the principles of sustainable development. The economic significance of the self cleaning   textiles can be outlined as follows:
1.   Ease of maintenance and environmental protection because of reduced cleaning efforts
2.   Time, material, energy reduction and consequently cost-efficiency during       production
3.   Reduced requirements regarding static properties by weight reduction at construction textiles
4.   Fuel savings through weight reduction in the field of transport
5.   Improved ageing behavior by extended surface purity effect.

REFRENCES


  1. A new dimension to textiles/garments - Pradeep Kaira,
  2. http://www.snaimpex.com/a_new_dimension_to_textiles.htm.
  3. Hatch KL: Making a claim that a garment is UV protective.
  4. AATCC Review,3, (2003),23-26.
  5. Development of New Textile Processing Technology Based on Nano-
  6. Technology-Nano-Scale Coating Made Possible on Monofilament                                                                                                                                                                                                                           Surface,                                
  7. http://www.toray.com/news/fiber/nr041022.html
  8. Selected Applications of Nanotechnology in Textiles, Y. W. H. Wong, etal..AUTEX Research Journal, Vol. 6, No 1, March 2006.

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